The influence of technological parameters asymmetric rolling on the physics and mechanical properties of titanium powder sheets
Abstract
Gogaev K., Voropaev V., Podrezov Yu., Minakov M., Vdovychenko O. The influence of technological parameters asymmetric rolling on the physics and mechanical properties of titanium powder sheets
To work out optimal technological modes of asymmetric rolling for obtaining titanium powder sheets. with maximum raw strength, a complex approach was used, which involves the study of the influence of several technological factors: deformation scheme (symmetric and asymmetric rolling), rolling temperature, force on the rolls and protective medium. The studies have shown that asymmetrical rolling method allows to significantly improve the mechanical properties of titanium powder sheets compared to symmetric rolling due to the shear component of the deformation, which improves the conditions of contact formation at the inter-particle boundaries. The optimal conditions asymmetric rolling for obtanong strengtyning titanium sheets are: a temperature interval of the rolling process Tr = 200-400 oC and a pressing force N ~100 kN. Under these conditions, the powder sheets demonstrate the highest green strength in the range σf = 800 MPa and dynamic characteristics approaching the values characteristic of compact titanium. After asymmetric rolling at 200 oC, the sheets have the highest hardness Нμ = 200-215 MPa. This value is significantly higher than that of recrystallized titanium, but is significantly inferior to the values of microhardness obtained on titanium samples deformed by severe plastic deformation methods. Relatively low hardness, as well as the invariance of the geometric dimensions of the sheets after different modes of deformation, indicates the local nature of intense shear at the interparticle boundaries, which enhances the process of contact formation The use of a protective atmosphere allows to increase strength and plasticity but the sheets remained relatively brittle, their maximum deformation before failure did not exceed ε= 1.5 %.
References
Podrezov Yu. N., Evich Ya.I. Verbylo D. G. The role of shear deformations in the consolidation of powder materials. Physics and technology of high pressures. 2014. V. 24, № 1. С. 98–109. (in Russian).
Podrezov Yu. N., Nazarenko V.A., Yevych Ya.I. Маrchenko N.M. Study of the regularity of contact formation in metal powder materials based on the results of precision mechanical tests. . Electron microscopy and strength of materials К.: IPMS № 16, 2014. С. 157–163. (in Ukrainian).
Gogaev K.A., Voropaev V.S., Podrezov Yu.N.,. Lugovskoi Yu.F, Nazarenko V.A., Koval A.Yu., and Yevych Ya.I.,, “Mechanical and fatigue properties of powder titanium strips, obtained by asymmetric rolling”, Powder Metall. Met. Ceram., 56, 53-59 (2017).
Kalutskii G.Ya., Gogaev K.A., Voropaev V.S. and Nepomnyashchii V.V., “Asymmetric rolling of metal powders and granules”, Powder Metall. Met. Ceram., 46, 197–201 (2007).
Gogaev K.A., Kalutskii G.Y. and Voropaev V.S., Asymmetric rolling of metal powders. II. Angular parameters of asymmetric rolling. Powder Metall. Met. Ceram. 48, 274–278 (2009).
Voropaev V.S. Effect of Mismatch in Asymmetric Rolling of Powders on the Plot of Total Normal Contact Stress. Technological systems. 2012. № 4(61). C. 28–30. (in Russian).
Gogaev K. A., Voropaev V. S., Podrezov Yu. N., Evich Ya.I. and Koval’ A.Yu., “The effect of compacting rolling on the properties of titanium powder mill products”, Powder Metall. Met. Ceram., 55, No. 11, 633–639 (2017).
Stern M. B., Beigelzimer Ya. E., Mikhailov O. V., and Synkov A. S. Twist extrusion of powder blanks. II. Experiment and discussion of results. Physics and technology of high pressures. 2008. V. 18, No. 3. S. 92–98. (in Russian)
Stern M. B., Beigelzimer Ya. E., Epifantseva T.A. Synkov A. S. Obtaining unsintered heterogeneous composite materials by screw extrusion. Physics and technology of high pressures. 2009. V. 19, No. 3. S. 120 –124. (in Russian)
Beygelzimer Y.E., Pavlenko D.V., Synkov O.S. and Davydenko O.O., “The efficiency of twist extrusion for compaction of powder materials”, Powder Metall. Met. Ceram., 58, 7–12 (2019).
Timoshenko S., Young D.H., Weaver W., Jr., Vibration Problems in Engineering, Wiley, 1974, 472p.
Gogaev K.A., Voropaev V.S., Vdovychenko O.V., Podrezov Yu.N.,. Gadzyra N.F, Yevich Ya.I. “The influence of deformation modes on the structure and properties of Al-Mg-X powder composites I. The influence of rolling conditions on the mechanical properties of aluminum powder ribbons strengthened with SiC nanoparticles” Powder Metall. Metal Ceramics, 57, 257-264 (2018).
Katashinskii V.P. and Shtern M.B. “Stressed-strained state of powder being rolled in the densification zone. I. Mathematical model of rolling in the densification zone”, Powder Metall. Met. Ceram., 22, 11, 882-885 (1983).
Kotko A.V., Moiseev V.F., Moiseeva I.V. Formation of dislocation structures and mechanical properties of a-titanium in the range from –196 to 850 °С. Metallophysics and the latest technologies. 1997. V. 19, No. 4. S. 50. (in Russian)
Clouet E., Caillard D., Chaari N., Onimus F. and. Rodney D. Dislocation locking versus easy glide in titanium and zirconium. Nature materials. September 2015.Vol 14. pp.931-937 www.nature.com/naturematerials DOI: 10.1038/NMAT4340
Cheng J. and Nemat-Nasser S. A Model for experimentally observed high strain rate dynamic strain aging in titanium. Acta mater. 48 (2000) 3131-3144.